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Controlled current bulk electrolysis is analogous to chronopotentiometry, the major difference being the use of larger area electrodes in bulk electrolysis. Users are directed to the wiki regarding chronopotentiometry for a more detailed description regarding setup, theory and application. Links: Electrochemist's Guide, AfterMath User's Guide, AfterMath Main Support Page Related Techniques: Chronopotentiometry (CP), Controlled Potential…

The choice of measurement sensitivity is very important when performing an electrochemical technique. If the instrument sensitivity is set too low, then small signals may be lost in the noise. If the instrument sensitivity is adjusted too high, then even relatively small signals may overwhelm the measurement circuitry, causing large features in the signal to…