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Organic Electrochemistry Short Course
Organic Electrochemistry Short Course
Workshop Date(s)
15 - 16 August 2019
Registration
Workshop Archived

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External Website

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Host Institution
University of Wisconsin-Madison
Department of Chemistry
Location
Topics
  • constant current electrolysis
  • constant potential electrolysis
  • cyclic voltammetry
  • organic electrosynthesis
Workshop Description

A two day electrochemistry workshop focused on organic electrochemistry including both theory and hands on experimentation.

Workshop Team
Shannon Stahl (PhD)
Professor of Chemistry
University of Wisconsin - Madison
Host, Co-Organizer, Lecture Faculty, Laboratory Faculty
Mohammad Rafiee (PhD)
Assistant Professor
University of Missouri - Kansas City
Co-Organizer, Lecture Faculty
Tim Paschkewitz (PhD)
Principal Electrochemical Sales Scientist
Pine Research Instrumentation
Co-Organizer, Laboratory Faculty, Teaching Assistant, Sponsor
Workshop Schedule
15 August 2019
Time
Location
Event
Details
Team Lead(s)
09:00
Room 1315
Lecture 1: Introduction to Electro-organic Chemistry and Chemical Organic Synthesis
Shannon Stahl
09:55
Room 1315
Lecture 2: Principles of Electron Transfer at Electrodes: Thermodynamic Considerations, Mass Transport and Introduction to Cyclic Voltammetry
Mohammad Rafiee
10:45
Break
11:00
Room 1315
Lecture 3: Applications of Electrochemical Organic Synthesis-I
Shannon Stahl
12:00
Lunch
13:15
Room 1315
Lecture 4: Constant Potential and Constant Current Experiments: Analytical and Bulk Electrolysis Methods
Mohammad Rafiee
14:30
Laboratory 1
2:30 - 4:00, Bulk Electrolysis: Shono-oxidation under constant potential and constant current 4:00 - 5:00, Bulk Electrolysis: Iodide-mediated benzylic C-H oxidation - preparation of benzylpryidinium
16 August 2019
Time
Location
Event
Details
Team Lead(s)
09:00
Laboratory 2: Q&A and troubleshooting electrolysis reactions
09:45
Room 1315
Lecture 5: Applications of Electrochemical Organic Synthesis - II (Indirect Electrolysis)
Shannon Stahl
10:45
Break
11:00
Room 1315
Cyclic Voltammetry and Chronoamperometry: Applications and Mechanistic Studies
Mohammad Rafiee
12:00
Room 9341
Lunch
Working lunch for lab participants, TAs, instructors, Pine/AbbVie representatives
13:15
Laboratory 3
1:15 - 3:00, Voltammetric and chronoamperometric experiments
15:00
Break
15:15
Troubleshooting and Data Analysis of Voltametric Experiments
17:00
Workshop concludes
Workshop Photo Gallery
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