Pine Research MSR Rotator with Glassy Carbon RDE

Pricing

#	Description	Price in USD
MSR Rotating Disk Electrode (RDE) Bundle
[MSR-RDE-E5TQ]	MSR ChangeDisk Rotating Disk Electrode Bundle features E5TQ series ChangeDisk RDE tip with interchangeable glassy carbon disk includes MSR Rotator, shaft, electrodes, cell, and accessories
Power Cord	this bundle includes one power cord
List of All Items Included in Bundle
AFMSRCE	Pine Research MSR Rotator includes motor control unit the most popular electrode rotator in the world
AFE5TQ050PK	ChangeDisk RDE Tip 15.0 mm OD PEEK shroud, PTFE U-Cup insulator accepts 5.0 mm OD disk inserts maximum rotation rate is 2500 RPM - never exceed maximum rotation rate when working with rotating electrodes.
AFED050P040GC	Glassy Carbon Disk Insert 5.0 mm OD x 4.0 mm L please read our glassy carbon disclaimer
AFE6K050	Disk Ejection and Polishing Tools for use with E5TQ and E6R1 ChangeDisk tips tools for installing, removing, and polishing disk inserts
AFE6MB	RDE/RRDE Shaft for MSR Rotators precision 15.0 mm OD PEEK shroud, stainless steel rod
AFCTR5	Standard Platinum Counter Electrode Kit 6.9 mm OD epoxy tube shroud, 150 mm long, includes fritted isolation tube
RREF0021	Single-Junction Silver Chloride (Ag/AgCl) Reference Electrode includes 14/20 PTFE adapter, storage bottle, bottle of filling solution
AKCELL3	Jacketed Glass Cell for Rotating Electrodes includes five PTFE stoppers, gas vent bend, and dual-port gas sparge tube
AC01TPA6M	Gas-Purged Bearing Assembly helps center rotating shaft within the 24/25 center port on the glass cell
AKPOLISH	Polishing Solutions and Materials Kit this kit includes three packs of polishing disks (microcloth, nylon, and 600 grit sandpaper) and three bottles of polishing solutions (5.0 µm, 0.3 µm, and 0.05 µm)

Description

This bundle includes an E5TQ series ChangeDisk RDE tip with an interchangeable glassy carbon disk insert. As your research grows, you can expand your rotating electrode collection to include a wide variety of additional RDE, RCE and RRDE tip designs that are compatible with the Pine Research MSR Rotator.

MAXIMUM ROTATION RATE: Each electrode tip model used with the Pine Research MSR Rotator has a maximum rotation rate. Do not the exceed maximum rotation rate when working with rotating electrodes.

The Pine Research MSR Rotator is the most popular rotating electrode configuration worldwide. This flexible electrochemical instrument may be used with Rotating Disk Electrodes (RDE), Rotating Ring-Disk Electrodes (RRDE), and Rotating Cylinder Electrodes (RCE). The MSR Rotator bears both the CE and ETL marks and is compatible with most international power configuration standards.

The rotation rate of the electrode may be adjusted using a control knob on the front panel of the motor control unit, or alternately, the rotation rate can be controlled via an analog control signal provided by a potentiostat or by a third-party waveform generator. The rotation rate may be viewed using the LCD display on the front panel. The rotation rate is adjustable over a range from 50 to 10,000 RPM and is accurate to within 1% of the reading on the display. A rotation rate may also be monitored via an output signal proportional to the rotation rate which is available on the front panel.

The rotation rate may be controlled and modulated by a sine wave, square wave, or other externally generated waveform. The outstanding acceleration characteristics of the motor and its control circuitry allow the rotation rate to follow the control waveform with very little error. This feature is particularly desirable for techniques such as Hydrodynamic Modulation Voltammetry (HMV) .

The rotator motor position is easily raised or lowered with respect to the cell platform, making immersion or removal of the rotating electrode tip quick and easy. The enclosure base is made from chemically resistant polypropylene, and the large enclosure window provides a good view of rotating electrode during operation. (A smaller base is available separately for using the rotator in a glove box or fume hood.)

Electrode connections are made to the rotating shaft using silver-carbon brushes. There are two contacts – the red is for the disk, and the blue is for the ring.

Visit our YouTube channel for helpful instructional videos regarding the use and maintenance of this and many other Pine Research products.

Pine Research YouTube

Specification

All specifications are subject to change without notice.


Modulated Speed Rotator (MSR)
Rate Accuracy	100 to 200 RPM: Accurate to within ±2 counts of display reading 200 to 10,000 RPM: Accurate to within ±1% of display reading
Rate Control (external)	Optional rate control via input signal on control unit front panel Available control ratios: 1, 2, or 4 RPM/mV, jumper selectable
Rate Output	Allows optional external monitoring of rotation rate (banana jack, control unit front panel) Output signal ratio: 1 RPM/mV (±1%)
Maximum Continuous Torque	28.3 mN m
Motor Power	15 W
Electrode Connections	Disk electrode: red banana jack on motor unit Ring electrode: blue banana jack on motor unit
Dimensions	Control unit: 11.4 × 10.1 × 5.75 in (29 × 26 × 15 cm) Rotator enclosure: 18.8 × 15.5 × 21.0 in (48 × 40 × 54 cm)
Shipping Information	Shipping weight: 60 lb (27 kg) Shipping dimensions: 24.0 × 24.0 × 24.0 in (61 × 61 × 61 cm)
Rotating Disk (RDE)	E2, E3, E4TQ, E5, E5TQ
Rotating Ring-Disk (RRDE)	E6, E7, E8
Rotating Cylinder (RCE)	ACQC, E9
Additional Specifications	click here for a complete list of specifications
Single Junction Silver Chloride Reference Electrode
Standard Potential	0.199 V vs. NHE
Filling Solution	4 M KCl with AgCl

Documentation

Document #	Title
Pine Research MSR Rotator
DRU10002	Pine Research MSR Rotator User Guide click here to download (6 MB download)
DRB10087	Pine Research MSR Rotator Marketing Brochure click here to download (951 KB download)
Electrode Information
DRP10143	E5TQPK Series ChangeDisk Rotating Disk Electrode Information click here to download (1 MB download)
DRP10061	Care and Use of the Platinum Counter Electrode Kit click here to download (252 KB download)
DRP10025	Silver/Silver-Chloride Reference Electrode User Guide click here to download (333 KB download)
DRK10135	Electrode Shrouds Overview click here to download (177 KB download)
DRK10013	Pine Research Electrode Polishing Guide click here to download (239 KB download)

Support

Below are selected product references:


Modulated Speed Rotator (MSR) [AFMSRCE]
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Schmies, H. ; Hornberger, E. ; Anke, B. ; Jurzinsky, T. ; Nong, H. N. ; Dionigi, F. ; Kühl, S. ; Drnec, J. ; Lerch, M. ; Cremers, C. ; Strasser, P. Impact of Carbon Support Functionalization on the Electrochemical Stability of Pt Fuel Cell Catalysts. Chem. Mater., 2018, 30(20), 7287-7295. Qi, J. ; Zhang, W. ; Xu, L. Solvent-Free Mechanochemical Preparation of Hierarchically Porous Carbon for Supercapacitor and Oxygen Reduction Reaction. Chemistry – A European Journal, 2018, 24(68), 18097-18105. Li, B. ; Wang, J. ; Gao, X. ; Qin, C. ; Yang, D. ; Lv, H. ; Xiao, Q. ; Zhang, C. High performance octahedral PtNi/C catalysts investigated from rotating disk electrode to membrane electrode assembly. Nano Res., 2019, 12(2), 281-287. Adhikary, S. D. ; Tiwari, A. ; Nagaiah, T. C. ; Mandal, D. Stabilization of Cobalt-Polyoxometalate over Poly(ionic liquid) Composites for Efficient Electrocatalytic Water Oxidation. ACS Appl. Mater. Interfaces, 2018, 10(45), 38872-38879. 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Precision 15 mm RDE/RRDE Shaft [AFE6MB]
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Standard Platinum Counter Electrode [AFCTR5]
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Single Junction Silver Chloride Reference Electrode [RREF0021]
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RDE/RRDE Cell With Water Jacket [AKCELL3]
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Electrode Polishing Kit [AKPOLISH]
San Roman, D. ; Krishnamurthy, D. ; Garg, R. ; Hafiz, H. ; Lamparski, M. ; Nuhfer, N. T. ; Meunier, V. ; Viswanathan, V. ; Cohen-Karni, T. Engineering Three-Dimensional (3D) Out-of-Plane Graphene Edge Sites for Highly Selective Two-Electron Oxygen Reduction Electrocatalysis. ACS Catal., 2020, 10(3), 1993-2008.

MSR Rotator ChangeDisk RDE Bundle (E5TQ)

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MSR Rotator ChangeDisk RDE Bundle (E5TQ)

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